TY - JOUR
T1 - Simple Setup Miniaturization with Multiple Benefits for Green Chemistry in Nanoparticle Synthesis
AU - Mathiesen, Jette K.
AU - Cooper, Susan R.
AU - Anker, Andy S.
AU - Kinnibrugh, Tiffany L.
AU - Jensen, Kirsten M.Ø.
AU - Quinson, Jonathan
N1 - Funding Information:
This project has received funding from the European Union’s Horizon 2020 research and innovation program under the Marie Sklodowska-Curie grant agreement No. 840523 (CoSolCat, JQ) and 841903 (SRC). This project has received funding from the Villum Foundation through a Villum Young Investigator grant (VKR00015416) and the Danish National Research Foundation (DNRF 149) Center for High-Entropy Alloy Catalysis (CHEAC). This research used resources of the Advanced Photon Source, a U.S. Department of Energy (DOE) Office of Science User Facility, operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357 (GUP-73929).
Publisher Copyright:
© 2022 The Authors. Published by American Chemical Society.
PY - 2022
Y1 - 2022
N2 - The development of nanomaterials often relies on wet-chemical synthesis performed in reflux setups using round-bottom flasks. Here, an alternative approach to synthesize nanomaterials is presented that uses glass tubes designed for NMR analysis as reactors. This approach uses less solvent and energy, generates less waste, provides safer conditions, is less prone to contamination, and is compatible with high-throughput screening. The benefits of this approach are illustrated by an in breadth study with the synthesis of gold, iridium, osmium, and copper sulfide nanoparticles.
AB - The development of nanomaterials often relies on wet-chemical synthesis performed in reflux setups using round-bottom flasks. Here, an alternative approach to synthesize nanomaterials is presented that uses glass tubes designed for NMR analysis as reactors. This approach uses less solvent and energy, generates less waste, provides safer conditions, is less prone to contamination, and is compatible with high-throughput screening. The benefits of this approach are illustrated by an in breadth study with the synthesis of gold, iridium, osmium, and copper sulfide nanoparticles.
U2 - 10.1021/acsomega.2c00030
DO - 10.1021/acsomega.2c00030
M3 - Journal article
C2 - 35155963
AN - SCOPUS:85124138467
VL - 7
SP - 4714
EP - 4721
JO - ACS Omega
JF - ACS Omega
SN - 2470-1343
IS - 5
ER -