Structural and physicochemical characterization of modified starch from arrowhead tuber (Sagittaria sagittifolia L.) using tri-frequency power ultrasound

Husnain Raza, Kashif Ameer, Haile Ma, Qiufang Liang*, Xiaofeng Ren

*Corresponding author for this work

Research output: Contribution to journalJournal articleResearchpeer-review

36 Citations (Scopus)

Abstract

Sagittaria sagittifolia L. is a well-known plant, belongs to the Alismataceae family. Sonication can improve the functional properties of starch; hence, the aim of this study was to develop ultrasonically modified arrowhead starch (UMAS) using a sophisticated and eco-friendly tri-frequency power ultrasound (20/40/60 kHz) method at 300, 600, and 900 W for 15 and 30 min. Significant (p < 0.05) increases in swelling power, solubility, and water and oil holding capacities were achieved. FTIR spectroscopy corroborated the ordered, amorphous, and hydrated crystals of the sonicated samples. Increases in sonication frequency and power led to significant (p < 0.05) increases in onset gelatinization temperatures. Scanning electron microscopic analysis of sonicated samples showed superficial cracks and roughness on starch granules appeared in a sonication power-dependent manner compared with that of untreated sample. Overall, the ultrasonically-treated samples showed improved physicochemical properties, which could be useful for industrial applications.

Original languageEnglish
Article number105826
JournalUltrasonics Sonochemistry
Volume80
ISSN1350-4177
DOIs
Publication statusPublished - Dec 2021

Bibliographical note

Funding Information:
The authors wish to express their appreciation for the support obtained from 643 the National Natural Science Foundation of China (Grants No. 31771977& 32072355 ); 644 The Jiangsu agricultural science and technology innovation fund (Grants No. 645 CX(20)3044 ); The Primary Research & Development Plan of Zhenjiang (Grants No. 646 NY2020011 ); Sponsored by Qing Lan Project (2020); Jiangsu Province Postdoctoral 647 Science Foundation Special Funding Project (2019K114); Priority Academic Program 648 Development of Jiangsu Higher Education Institutions (PAPD).

Publisher Copyright:
© 2021 The Authors

Keywords

  • Arrowhead
  • Modified starch
  • Morphology
  • Physicochemical characterization
  • Ultrasound

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